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THERMO JARRELL ASH, ATOMIC VAPOR ACCESSORY, MODEL NO.- 4. DATE- 1. 0/9. 5, V- 1. AMPS- 3, HZ- 5. 0/6. S/N- 2. 78. 5, PHASE- 1, W/ PYREX #5. ML. FLEAKER BOTTLE, W/ PYREX #5. ML. FLEAKER BOTTLE ,W/ PYREX #5. ML FLEAKER BOTTLE. THERMO JARRELL ASH FURNACE ATOMIZER 1. MODEL NO.- 1. 88, DATE- 5/9. V- 2. 08, AMPS- 2. HZ- 6. 0, S/N- 2. PHASE- 1. HEWLETT PACKARD 5. B FT- IR INFRARED DETECTOR, S/N: 2. A0. 02. 02, M/N: 5. B, 1. 00- 1. 20, 2. V, 4. 8- 6. 6HZ. BIO- RAD DIGILAB DIVISION FTS- 4. FT- IR WITH MICROSCOPE, 1 S/N: 0. UMA - 3. 00. A 1. A. C. VOLTS: 6. 0 HZ 1. A OLYMPUS #0. F3. WITH EA4 0. 1. 0. LENS WITH POWER SCN A/D BIO RAD DIGI LAB DIVISION, FTS - 4. M/C WITH BIO RAD MODEL FTS- 4. S/N: 3. 07. 30 1. A. C. MATTSON INSTRUMENTS INC, 7. GALAXY SERIES FT- IR 7. MODEL: GL- 7. 02. S/N: 9. 30. 83. 8G, VOLTS1. HZ, 1. 99. 6 FIRMWARE VERSION 8. WORKING CONDITION NO ERROR MESSAGES HOWEVER SCREEN VERY HARD TO READ. MATTSON INSTRUMENTS 4. GALAXY SERIES FT- IR MODEL GL- 4. S/N 9. 00. 71. 1G 1. V 6. 0HZ 5. A. MATTSON INSTRUMENTS GALAXY 2. SERIES FT- IR MODEL: GL- 2. S/N: 9. 01. 12. 2G, VOLTS: 1. HZ. PERKIN ELMER 5. ATOMIC ABSORPTION SPECTROPHOTOMETER. MISSING PARTS SOLD FOR PARTS OR REPAIR. PERKIN ELMER 5. 10. ZL ZEEMAN FURNACE MODULE ID NR. WITH PERKIN ELMER AS 7. AUTO SAMPLER ID NR. INCLUDES PERKIN ELMER GEM SOFTWARE AND DELL COMPUTER WITH MONITOR, KEYBOARD, MOUSE AND FLAT SCREEN MONITOR, AND NATIONAL INSTRUMENTS GPIB- USB- HS COMPUTER INTERFACE. SOFTWARE IS LOADED ON COMPUTER AND COMPUTER TALKS TO THE FURNACE AND AUTO SAMPLER. FURNACE HAS BROKEN GLASS ON THE SIDE SEE PHOTOS. PERKIN ELMER 5. 10. ZL ATOMIC ABSORPTION SPECTROMETER FOR PARTS ONLY WITH PERKIN ELMER 5. ZL ZEEMAN FURNACE MODULE ID NR. WITH PERKIN ELMER AS 7. AUTO SAMPLER ID NR. INCLUDES PERKIN ELMER GEM SOFTWARE AND DELL COMPUTER WITH MONITOR, KEYBOARD, MOUSE AND FLAT SCREEN MONITOR, AND NATIONAL INSTRUMENTS GPIB- USB- HS COMPUTER INTERFACE. SOFTWARE IS LOADED ON COMPUTER AND COMPUTER TALKS TO THE FURNACE AND AUTO SAMPLER. FURNACE HAS BROKEN GLASS ON THE SIDE SEE PHOTOS. PERKIN ELMER FURNACE COOLING SYSTEM, ID NR# 1. SERIAL# 3. 08. 4, 2. V, 5. 0/6. 0V, 5. HZ, 6. 5VA. PERKIN ELMER SPECTRUM TWO FT- IR SPECTROMETER, WITH SINGLE CELL HOLDER. S/N: C9. 41. 29, MODEL: L1. WITH DELL LAP TOP COMPUTER, WITH WINDOWS 7 OPERATION SYSTEM AND PERKIN ELMER ENVIRONMENTAL HYDROCARBON FT- IR TOUCH APPS SOFTWARE CD LX1. A, 1. 1/0. 8/1. 1. INCLUDES 1) 4. CM- 1 @ 4. CM SLIDE, 1) 0. 5. CM- 1 @ 4. 00. 0 CM SLIDE, 1) 2. CM- 1 @ 4. 00. 0 CM SLIDE, 1) HALF APERTURE SLIDE, 1) 1. CM- 1 @ 4. 00. 0 CM SLIDE, AND 2) PERKIN ELMER UV- VIS SPECTROSCOPY CELLS P/N: B0. MM WITH LIDS. DETERMINATION OF HYDROCARBONS IN ENVIRONMENTAL SAMPLES WITH SPECTRUM TWO INTRODUCTION THE CONCENTRATION OF DISPERSED OIL AND GREASE IN WATER IS AN IMPORTANT PARAMETER FOR HUMAN AND ENVIRONMENTAL HEALTH. INFRARED SPECTROSCOPY HAS LONG BEEN A STANDARD METHOD FOR DETECTING AND QUANTIFYING HYDROCARBON CONTAMINATION, PARTICULARLY IN WATER DISCHARGED DURING OFFSHORE OIL OPERATIONS. RECENTLY, THIS ANALYTICAL TECHNIQUE HAS ENJOYED RENEWED INTEREST AND APPLICATION TO A WIDER RANGE OF ENVIRONMENTAL SAMPLES AND MATRICES, FROM COOLING WATER, TO SOIL IN LAND RECLAMATION, TO DRINKING WATER; AT THE SAME TIME, CONCERN OVER THE ENVIRONMENTAL IMPACT OF CHLOROFLUOROCARBON SOLVENTS HAS LED TO THE DEVELOPMENT OF A NUMBER OF ALTERNATIVE APPROACHES USING LESS HARMFUL SOLVENTS. THIS APPLICATION NOTE PRESENTS AN OVERVIEW OF THREE METHODS AND A COMPARISON OF THEIR PERFORMANCE: 1. HALOGENATED SOLVENT EXTRACTION AND TRANSMISSION MEASUREMENT (C- H STRETCH MODES), E. G. THIS IS THE TRADITIONAL APPROACH, BUT REQUIRES THE USE OF RELATIVELY EXPENSIVE SOLVENTS THAT MAY BE HARMFUL. HEXANE EXTRACTION AND ATR MEASUREMENT ALLOWS THE USE OF AN INEXPENSIVE HYDROCARBON SOLVENT, BUT DOES NOT PERMIT THE MEASUREMENT OF VOLATILE CONTAMINANTS. CYCLOHEXANE EXTRACTION AND TRANSMISSION MEASUREMENT (1. CM- 1) EXPLOITS A DEFORMATION MODE THAT IS NOT PRESENT IN THE SPECTRA OF CYCLOALKANES (SEE FIGURE 1), AND COMBINES THE SIMPLICITY OF A TRANSMISSION MEASUREMENT WITH A HYDROCARBON SOLVENT. ALL THREE OF THESE METHODS ARE SUPPORTED BY THE SPECTRUM TWO ENVIRONMENTAL HYDROCARBONS ANALYSIS SYSTEM (FIGURE 2), WITH THE APPROPRIATE SAMPLING ACCESSORY. THIS NOTE EVALUATES THE THREE METHODS AND DISCUSSES THEIR RELATIVE ADVANTAGES. PERKIN ELMER, FT- IR SPECTROMETER, SPECTRUM 2. S/N- 4. 74. 87, DATE OF MANUFACTURE- 1. PARTS UNIT photo. QTY. PERKIN ELMER FT- IR SPECTROMETER SPECTRUM RX- 1 S/N: 7. DATE OF MFG 2/2/0. PART # L1. 18. 52. V 1. 20. V/2. 20. V 2. 5 AMP MAX FUSE 3. AT. PERKIN ELMER FT- IR SPECTROMETER SPECTRUM RX1 SER 6. DATE OF MANUFACTURE 0. PN L 1. 18. 52. 47 1. V 1. 20. V- 2. 20. V 2. 40. V 2. 5 AMP MAX FUSE 3. AT. PERKIN ELMER SPECTRUM RX 1 FT- IR SYSTEM SER 5. DATE OF MANUFACTURE 0. PN L1. 18. 52. 47 1. V 1. 20. V- 2. 20. V 2. 40. V 2. 5. 55. AMP MAX FUSE 3. 1. AT. PERKIN ELMER FT- IR SPECTROMETER SPECTRUM 2. S/N: 4. 26. 20 DATE MFG SEPT 1. S/N: 4. 26. 19 MODEL NAME SPECTRUM 2. POWER SUPPLY TAKEN OUT. PARTS UNIT photo. QTY. PERKIN ELMER FT- IR SPECTROMETER PARAGON 1. V/2. 20- 2. 40. V 2. A MAX 5. 0/6. 0 HZ P/N L1. F1. 41 S/N 3. 86. PERKIN ELMER FLOW INJECTION MERCURY SYSTEM MODEL: FIAS 1. ID#: 5. 09. 55. 0, S/N: 1. VAC, 5. 0/6. 0HZ, 4. VA, FRONT WORK TRAY 5. NICOLET 5. 60 ESP FT- IR SPECTROMETER TYPE: MAGNA IR 5. S/N: ADU9. 80. 04. VAC, 5. 0/6. 0HZ, 1. WATTS. NICOLET 5. PC FT- IR SPECTROMETER, BEAM 5. PC, S/N: 8. 90. 04. VAC, 5. 0/6. 0HZ, . NICOLET IMPACT 4. D FT- IR (FOURIER TRANSFORM INFRARED) SPECTROPHOTOMETER, MODEL: IMPACT, S/N: ACM9. VOLT, photo. QTY. VARIAN SPECTRA A- 4. ZEEMAN ATOMIC ABSORPTION SPECTROMETER, 2. V, 2. 20. V, 2. 40. V, W/ VARIAN ZEEMAN GRAPHITE TUBE, ATOMIZER, 2. V, 2. 20. V, 2. 40. V. VARIAN GTA- 9. GRAPHITE TUBE ATOMIZER, S/N: 9. VARIAN SPECTRA AA- 3. PLUS ATOMIC ABSORPTION SPECTROPHOTOMETER, S/N: 9. ALLIED ANALYTICAL SYSTEMS / INSTRUMENTATION LABORATORY / THERMO JARRELL ASH, VIDEO 1. E AA/AE SPECTROPHOTOMETER, MODEL 7. S/N 1. 93. 7, DATE: 7/8. ALLIED ANALYTICAL SYSTEMS / INSTRUMENTATION LABORATORY S- 1. AA/AE SPECTROPHOTOMETER. THE IL S- 1. 1 IS A SINGLE CHANNEL, SINGLE BEAM AA/AE SPECTROPHOTOMETER. INSTRUMENT HAS AS STANDARD THE SMITH- HIEFTJE BACKGROUND CORRECTION SYSTEM AND A BUILT IN 8- BIT MICROCOMPUTER. INCLUDES OPERATOR'S MANUAL, AND ATOMIC ABSORPTION METHODS MANUAL VOLUME 1 STANDARD CONDITIONS FOR FLAME OPERATION, AND SERVICE MANUAL. PERKIN ELMER ATOMIC ABSORPTION SPECTROMETER MODEL: 4. S/N: 1. 02. 6, ID. N3. 05- 0. 70. 3, OPERATE 2. MAX. 3. 0, HAS ED1 AND ED2 PORT. INCLUDES SYSTEM DESCRIPTION MANUAL, SETTING UP AND PERFORMING FLAME ANALYSES MANUAL AND SETTING UP AND OPERATING GRAPHITE FURNACE ANALYSIS MANUAL,photo. QTY. PERKIN ELMER 4. ATOMIC ABSORPTION SPECTROMETER, MODEL: 4. ID NO.: 5. 05. 94. PERKIN ELMER ZEEMAN 5. S/N: 6. 93. 8 ID 5. V WITH PERKIN ELMER FURNACE MODEL: HGA 6. S/N: 5. 41. 1 2. 30. V, WITH MISC PARTS CONSISTING OF: THUMB SCREW 7. LIGHT (LED) 3. 40. DIALIGHT P/N: 1. 03- 3. PERKIN ELMER GEM DESKTOP SOFTWARE KIT S/N: 1. PERKIN ELMER BODENSEEWERK D7. UBERLINGEN S/N: 0. PERKIN ELMER HGA- 5. PROGRAMMER, S/N: 7. TYPE: HGA- 5. 00, WITH PERKIN ELMER GRAPHITE FURNACE, S/N: 2. ALSO INCLUDES SAMPLE TREY, S/N: 8. PERKIN ELMER ED1 SYSTEM 2, S/N: 6. FILE # W2. 33. 29. C, WITH PERKIN ELMER HGA COOLING SYSTEM, ID # 1. S/N: 3. 60. 4, WITH PERKIN ELMER HGA 6. WITH PERKIN ELMER EDI POWER SUPPLY S/N: 1. WITH PERKIN ELMER AS 6. SAMPLER, S/N: 8. 17. PERKIN ELMER / PE NELSON TURBOCHROM WORKSTATION 6. WITH VERSION 6. 1. CD WITH SUPPLEMENTARY DISK REV 6. WITH TURBOCHROM LC SYSTEM BACKUP 2 DISKS WITH TURBOCHROM QUICK REFERENCE GUIDE WITH LICENSE PAK LICENSE NAME PE LC IPM AUTHORIZATION 3. PERKIN ELMER/PE NELSON TURBOCHROM WORKSTATION 6. WITH VERSION 6. 0. CD WITH SUPPLEMENTARY DISK REV 6. WITH SUPPLEMENTARY DISK REV 6. SMR 1 WITH LICENSE PAK LICENSE NAME TURBO METHOD DEVELOPMENT AUTHORIZATION 3. PERKIN ELMER HS6 CONTROL A. ID- NR 0. 93. 30. S/N 2. 56. 7 B. PERKIN ELMER N2. BURNER. PERKIN ELMER HGA 6. S/N: 5. 69. 4 M/N: HGA- 6. P/N: BO 1. 26. 26. V 6. 0HZ. WITH PERKIN ELMER GRAPHITE FURNACE AND ELECTRO THERMAL VAPORIZATION SYSTEM S/N: 3. ID- NR. 1. 28. 58. WITH AUTO SAMPLER ACCESSORY AS- 6. S/N: 8. 64. 7 ID- NR. PERKIN ELMER EDL SYSTEM 2 SERIAL# 0. PART# N3. 05- 0. 60. ELEMENT: AS. PERKIN- ELMER INTENSITRON LAMP PART# 3. SERIAL# 1. 22. 87. CURRENT: CONTINUOUS 3. MA, 1. 2- 1. 5MA, ELEMENT: BE M- 2. W/ CASE. PERKIN- ELMER UNIVERSAL QTA BURNER MOUNT FOR ATOMIC ABSORPTION SPECTROMETER PAT# B3. NEW UN- OPENED. LIQUID SAMPLE STAGE FOR FT- IR. ATOMIC ABSORPTION BURNER HEAD 4 . AA LAMPS CONSISTING OF: QTY. FISHER SCIENTIFIC HOLLOW CATHODE LAMP PART NO. S/N B 3. 87. 07 ELEMENT BA GAS AR MAX CURRENT MA 2. QTY. FISHER SCIENTIFIC HOLLOW CATHODE LAMP PART NO. C S/N 6. 93. 54 ELEMENT FE GAS NE MAX CURRENT 1. MA QTY. FISHER SCIENTIFIC HOLLOW CATHODE LAMP PART NO. N S/N 6. 27. 79 ELEMENT CR GAS NE MAX CURRENT 1. MA QTY. FISHER SCIENTIFIC HOLLOW CATHODE LAMP PART NO 1. P S/N 7. 63. 41 ELEMENT AL GAS NE MAX CURRENT 1. MA QTY. FISHER SCIENTIFIC HOLLOW CATHODE LAMP PART NO 1. A S/N 7. 79. 68 ELEMENT CU GAS NE MAX CURRENT 5. MA QTY. FISHER SCIENTIFIC HOLLOW CATHODE LAMP PART NO 1. G S/N 8. 25. 69 ELEMENT CO GAS NE MAX CURRENT 1. MA QTY. FISHER SCIENTIFIC HOLLOW CATHODE TUBE CURRENT SETTING 8. CONTINUOUS MODE 6. MA 8. MA MAX MODULATED MODE 3. MA 1. 2MA MAX ELEMENT NA QTY. FISHER SCIENTIFIC HOLLOW CATHODE TUBE CURRENT SETTING 8. CONTINUOUS MODE 1. MA 2. 5MA MAX MODULATED MODE 7. 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